Mechanical characterization by CVD-FBR aliminium coatings on austenitic stainless steel and the steam oxidation resistance

Main Article Content

Autores

Diego Pérez-Muñoz
José Luddey Marulanda-Arévalo
Juan Manuel Meza-Meza

Abstract

The aluminum coatings deposited by Chemical Vapour Deposition Fluidisation (FBR-CVD) on the austenitic stainless steel AISI 317, show a more than 80 times corrosion rate reduction at high temperatures. The coatings mechanical characterization was conducted by means of microhardness, nano indentation, in order to konow how were affected the coating and the substrate’s mechanical properties (particularly the hardness and the Young’s modulus) after being subjected to oxidation at high temperature. Some analyses were also made by means of SEM, to observe the micro structural changes and to see how is the AFM topography and rugosity gradient variation, related to the distance traveled by the tip of the cantilever during the sweeps.

Keywords:

Article Details

Licence

All articles included in the Revista Facultad de Ingeniería are published under the Creative Commons (BY) license.

Authors must complete, sign, and submit the Review and Publication Authorization Form of the manuscript provided by the Journal; this form should contain all the originality and copyright information of the manuscript.

The authors who publish in this Journal accept the following conditions:

a. The authors retain the copyright and transfer the right of the first publication to the journal, with the work registered under the Creative Commons attribution license, which allows third parties to use what is published as long as they mention the authorship of the work and the first publication in this Journal.

b. Authors can make other independent and additional contractual agreements for the non-exclusive distribution of the version of the article published in this journal (eg, include it in an institutional repository or publish it in a book) provided they clearly indicate that the work It was first published in this Journal.

c. Authors are allowed and recommended to publish their work on the Internet (for example on institutional or personal pages) before and during the process.
review and publication, as it can lead to productive exchanges and a greater and faster dissemination of published work.

d. The Journal authorizes the total or partial reproduction of the content of the publication, as long as the source is cited, that is, the name of the Journal, name of the author (s), year, volume, publication number and pages of the article.

e. The ideas and statements issued by the authors are their responsibility and in no case bind the Journal.

References

R. Trevisan, C. Lima, Aspersao Termica Fundamentos E Aplicacoes. Brasil; Artliber. 2002.

J. L. Marulanda, S.I. Castañeda-Quintana, & A. Remolina-Millan, “Recubrimientos depositados por CVD-FBR para protección a alta temperatura”. Dyna; vol. 80, n.° 181, pp. 181-91. 2013.

J. Pérez-Mariano, J. Caro, C. Colominas. “Multilayer Coatings by Chemical Vapor Deposition in a Fluidized Bed Reactor at Atmospheric Pressure (Ap/Fbr-Cvd): Tin/Tan And Tin/W”. Surface & Coatings Technology. Elsevier, vol. 201, no. 6, pp. 2174-2180. 2006. Disponible en: http://www.sciencedirect.com/science/article/pii/S025789720600260X.

S. Hogmark, S. Jacobson y M. Larsson. Wear, vol. 246, pp. 20-33. 2000.

J. L. Marulanda-Arévalo, F. J. Pérez-Trujillo, & S. I. Castañeda-Quintana, “Behavior of aluminum coating by CVD-FBR in steam oxidation at 700 °C”. CT&F - Ciencia, Tecnología y Futuro, vol. 5, n.° 4, pp. 77-86. 2014.

J. Pérez-Mariano, K.H. Lau, A. Sanjurjo, J. Caro, D. Casellas, C. Colominas. “TiSiN nanocomposite coatings by chemical vapor deposition in a fluidized bed reactor at atmospheric pressure (AP/FBR-CVD)”, Surface and Coatings Technology, vol. 201, n.° 6, pp. 2217-2225, 2006.

J. L. Marulanda-Arévalo, F. J. Pérez-Trujillo y A. Remolina-Millán, “Recubrimientos de aluminio-silicio realizados por deposición química de vapor en lecho fluidizado sobre el acero inoxidable AISI 316”. Revista Facultad de Ingeniería, Uptc, Vol. 22, N.° 34. Enero-Junio de 2013.

P. Rodríguez, B. Caussat, C. Ablitzer, X. Iltis, & M. Brothier. “Fluidization and coating of very dense powders by Fluidized Bed Chemical Vapour Deposition”. Chemical Engineering Research and Design, vol. 91, pp. 2477-2483. 2013.

F.J. Pérez, F. Pedraza, M. P. Hierro and, P.Y. Hou, “Adhesion properties of aluminide coatings deposited via CVD in fluidised bed reactors (CVD-FBR) on AISI 304 stainless steel”, Surface & Coatings Technology, vol. 133-134, pp. 338-343. 2000. Disponible en: http://dx.doi.org/10.1016/S0257-8972(00)00952-X.

G. Angelopoulos, S. Kinkel, N. Voudouris, Surface and Coatings Technology, vol. 78, pp. 72-77. 1996.

J. L. Marulanda-Arévalo, S.I. Castañeda-Quintana y A. Remolina-Millán, “Oxidación en vapor de agua a 700 ºC y 750 ºC del acero inoxidable AISI 317 recubierto con aluminio por CVD-FBR”. Rev. Fac. Ing. Univ. Antioquia N.º 71, pp. 191-201. 2014.

D. Pérez-Muñoz, Nanocaracterización mecánica de recubrimientos de aluminio depositados sobre aceros inoxidables austeníticos sometidos a oxidación en vapor de agua. Tesis pregrado en Ingeniería Mecánica. Colombia. Universidad tecnológica de Pereira. Facultad de Ingeniería Mecánica. 2014.

M. Salerno, N. Patra & A. Diaspro. “Atomic force microscopy nanoindentation of a dental restorative midifill composite”. Dental Materials, vol. 28, pp. 197-203. 2012.

Electrical Mapping of AISI 304 Stainless Steel Subjected to Intergranular Corrison Performed by Means of AFM – L.

Y. Xia, M. Bigerelle, S. Bouvier, A. Lost, P.-E. Mazeran. Quantitative Approach to Determine the Mechanical Properties by Nanoindentation Test: Application on Sandblasted Materials. February 2015, pages 297-304.

Reza Pejman, S. Hassan Salehi, Manouchehr Salehi. “Numerical study of interfacial crack growth effects on Nanoindentation mechanical properties in presence of pre-existing defect”. October 2013, pp. 408-413.

Fisher-Cripps, Anthony C. Nanoindentation, Mechanical Engineering Series, 2nd edition, New York: Springer. 2012.

A. Stylianou & D. Yova. “Surface nanoscale imaging of collagen thin films by Atomic Force Microscopy”. Materials Science and Engineering, C, Materials for biological applications vol. 33, no. 5, pp. 2947–2957. 2013.

B. Destouches, Estudio del efecto del tamaño en nanoindentación. Tesis Maestría en Biomateriales. España. Universidad Politécnica de Cataluña. Departamento de Ciencia de los Materiales. 2008.

ASTM Standards, Estándar para ensayo de dureza Rockwell y dureza superficial Rockwell de materiales metálicos. ASTM E18-03.

Nanosurf. Easyscan 2 AFM Operating Instructions, SPM Control Software, versión 3.0. July 2011.

Image Metrology. SPIP Handbook, Control Software, version 6.2.6, 2014.

Qianhua Kan, Wenyi Yan, Guozheng Kang, Qingping Su. “Oliver – Pharr indentation method in determining elastic moduli of shape memory alloys – A phase transformable material”. Journal PF the Mechanics and Physics of Solids, Vol. 61, no. 10, pp. 2015-2033, October 2013.

L. E. Bertassoni, G. W. Marshall, M. V. Swain. “Mechanical heterogeneity of dentin at different length scales as determined by AFM phase contrast”. Micron, Vol. 43, no. 12, pp. 1364-1371, December 2012.

Downloads

Download data is not yet available.