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Vol. 27 No. 49 (2018)

Papers

Structural analysis of the JBW (Na-J, barrer and white) zeotype obtained from kaolinite-rich clay

https://doi.org/10.19053/01211129.v28.n49.2018.8545

Published 2018-08-07

  • Mario Alberto Macías-López, Ph. D.
    • ,
  • Carlos Alberto Ríos-Reyes, Ph. D.
    • ,
  • Oscar Mauricio Castellanos-Alarcón, Ph. D. (c)

Mario Alberto Macías-López, Ph. D.
Universidad Industrial de Santander

Carlos Alberto Ríos-Reyes, Ph. D.
Universidad Industrial de Santander

Oscar Mauricio Castellanos-Alarcón, Ph. D. (c)
Universidad de Pamplona

Abstract

The JBW zeolite was prepared from hydrogels under hydrothermal conditions by alkaline reaction, using NaOH as activating agent. The synthetic zeotype was studied by analytical techniques such as X-ray powder diffraction, scanning electron microscopy, Fourier transformed infrared spectroscopy and solid-state 29Si and 27Al Magic angle spinning nuclear magnetic resonance. Crystallographic data revealed that the JBW structure can be described by the orthorhombic space group Pna21, with unit cell parameters a=16.409(2) Å, b=14.966(2) Å and c=5.2154(5) Å.

Keywords

hydrogels, JBW structure, orthorhombic, space group, unit cell, zeotype

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